受賞国：日本国

受賞国：オランダ王国

受賞国：日本国

受賞国：日本国

受賞国：大韓民国

受賞国：日本国

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Science and Engineering: A  

The AlSi10Mg sample was additive-manufactured using laser powder bed fusion (L-PBF), and subsequent low-temperature annealing (LTA) at 413K or 473 K was applied. Vickers hardness tests show the peak at around 160 HV by 473 K annealing and around 145 HV by 413 K annealing. The flow stress of tensile and compression deformations are also affected by LTA, and peak aging condition gives the highest 0.2% proof stress. 0.2% proof stress obtained by tensile tests is around 270 MPa, whereas that obtained by compression tests is between 326 MPa and 386 MPa. Electrical resistivity at 293 K changes from approximately 80 nΩm down to around 60 nΩm, whereas that at 77 K changes from around 40 nΩm down to around 20 nΩm. The estimated concentration of solute Si in the as-built specimen is between 2.5 mass% and 2.9 mass%, corresponding to the previous results using energy-dispersive X-ray spectroscopy. The lattice constant obtained from XRD increased from 0.4043 nm up to 0.4048 nm by LTA. Both electrical resistivity and XRD measurement indicate a decrease in the concentration of solute atoms. Microstructure observations revealed numerous nano-sized precipitates of Si phase with a plate-like or granular morphologies in α-Al grains due to LTA.

DOI： 10.1016/j.msea.2023.144876

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Scripta Materialia  

Aluminum alloys fabricated by laser powder bed fusion (L-PBF) exhibit anisotropic tensile ductility. To identify microstructural origins in melt-pool (MP) structures (formed by the L-PBF process) contributing to the anisotropic ductility, the local strain distribution inside the MP structure in deformation was quantified by a combination of digital image correlation (DIC) strain analysis and in-situ SEM observations of tensile tests. It was found that higher strain was localized in locally coarsened microstructures (softer regions) along melt-pool boundaries (MPBs). The strain localization played a significant role in crack initiation (and propagation) around MPBs, contributing to fracture. The strain localization at MPBs changed depending on the geometrical relation of the MPBs with the loading direction (LD), which was controlled by the LD with respect to the building direction of L-PBF samples. The three-dimensional MPB distribution related to the LD would be responsible for the anisotropic ductility.

DOI： 10.1016/j.scriptamat.2022.115259

Scopus

担当区分：筆頭著者,　責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan  

This study was set to fundamentally investigate the characteristics of austenite reversion occurring in maraging steels additive-manufactured by laser powder bed fusion (L-PBF). The maraging steel samples manufactured under different L-PBF process conditions (laser power P and scan speed v) were subjected to heat treatments at 550°C for various durations, compared with the results of the austenitized and water-quenched sample with fully martensite structure. The L-PBF manufactured samples exhibited the martensite structure (including localized austenite (γ) phases) containing submicron-sized cellular structures. Enriched alloy elements were detected along the cell boundaries, whereas such cellar structure was not found in the water-quenched sample. The localized alloy elements can be rationalized by the continuous variations in the γ-phase composition in solidification during the L-PBF process. The precipitation of nanoscale intermetallic phases and the following austenitic reversion occurred in all of the experimental samples. The L-PBF manufactured samples exhibited faster kinetics of the precipitation and austenite reversion than the water-quenched sample at elevated temperatures. The kinetics changed depending on the L-PBF process condition. The enriched Ni element (for stabilizing γ phase) localized at cell boundaries would play a role in the nucleation site for the formation of γ phase at 550°C, resulting in the enhanced austenite reversion in the L-PBF manufactured samples. The variation in the reaction kinetics depending on the L-PBF condition would be due to the varied thermal profiles of the manufactured samples by consecutive scanning laser irradiation operated under different P and v values.

DOI： 10.2355/tetsutohagane.TETSU-2022-066

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Transactions  

In order to investigate the effects of Mn and Cu additions on solidification microstructure and high-temperature strength of cast AlFe alloys, we have fabricated various AlFe-based alloys with compositions of Al1%Fe, Al1%Fe1%Mn, Al1%Fe1%Cu, and Al1%Fe1%Cu1%Mn (mol%) solidified at different cooling rates (0.3 K·s11 and 145 K·s11). In the Al1%Fe binary alloy, the coarsened ª-Al13Fe4 phase with a needle-shaped morphology was often observed in the furnace-cooled sample (0.3 K·s11), whereas the cast sample (145 K·s11) exhibited several elongated ¡ phases surrounded by fine ¡/Al6Fe eutectic microstructure. Such a solidification microstructure was observed in the cast Al1%Fe1%Cu alloy, whereas the Al23CuFe4 phase was locally formed in the finally solidified zone in the furnace-cooled sample. In the Al1%Fe1%Mn alloy, the Al6(Fe, Mn) phase was formed regardless of the cooling rate. Finer ¡/Al6(Fe, Mn) two-phase eutectic microstructure was almost entirely occupied in the cast sample. The fine eutectic microstructure was observed in the cast Al1%Fe1%Cu1%Mn alloy as well. Compression tests for cast alloy specimens revealed that the Al1%Fe1%Cu1%Mn alloy exhibited the highest strength level among the studied alloy specimens, indicating the combined addition of Mn and Cu elements could be effective in improving the high-temperature strength of the cast AlFe alloys.

DOI： 10.2320/matertrans.MT-LA2022010

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Transactions  

The optimization of processing parameters is indispensable for the laser powder bed fusion (L-PBF) process. The deposited energy density (DED) is one of the process indexes for the L-PBF process and has a simplified formula of P v 0.5, where P is the laser power, and v is the scan speed. This parameter describes the change in the relative density and the melt pool morphology with laser power and scan speed well, whereas it does not include the effect of other processing parameters, e.g., hatch spacing (S). In the present study, an attempt was made to incorporate the effect of S into DED. Al12Si (mass%) alloy cube samples were fabricated by L-PBF under various P, v, and S, for evaluating the relative density and the melt pool morphology. The melt pool depth and width of L-PBF-manufactured Al12Si alloy increased linearly with P v 0.5 and did not exhibit a clear correlation with S. Based on the experimental observation, the effect of hatch spacing on DED was estimated to be S 0.5, and a new index of P v 0.5 S 0.5 was proposed. This index described the change in the relative density of the L-PBF-manufactured Al12Si alloy with laser conditions (P, v, and S) well when the thermal conduction mode melting was dominant. This study also indicated the limitation of the applicability of P v 0.5 S 0.5 under the keyhole or transition mode melting.

DOI： 10.2320/matertrans.MT-ME2022002

Scopus

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

The present study investigated the effect of trace titanium (Ti) addition on high-temperature creep properties of a heat-resistant quinary aluminum (Al) alloy, with a composition of Al-5Mg-3.5Zn-2Cu-2Ni (mol%). Both the quinary alloy and Ti-added alloy were solution-treated at 480°C and then aged at 200°C for 10 hours. The creep tests were conducted at 200°C under 105 MPa. The addition of trace Ti element reduced the minimum creep rate and delayed the onset of the tertiary creep stage (creep acceleration), resulting in the extended creep rupture life of the Al-5Mg-3.5Zn-2Cu-2Ni quinary alloy. The creep rupture life of the Ti-added alloy was higher than that of the A7075 alloy but lower than that of the A2618 alloy, whereas the initial creep rate (up to 0.2% in strain) of the Ti-added quinary alloy was lower than that of the A2618 alloy. The superior creep properties were presumably due to the enhanced stability of the fine precipitation morphologies of the T-Al6Mg11Zn11 phase by solute Ti inside the α-Al matrix.

DOI： 10.2464/jilm.73.260

Scopus

担当区分：筆頭著者,　責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Transactions  

In order to understand the influence of dislocation substructures on the size-dependent strength (smaller is stronger) of micron-sized metals, we have fabricated single-crystal cylindrical micropillars with various diameters approximately ranging from 1 to 10µm, which were prepared on the surface of the fully annealed sample and the subsequently cold-rolled samples of high-purity aluminum (Al). The annealed micropillars exhibited a size dependence of the resolved shear stress required for slip. The shear stress (¸i) normalized by shear modulus (G) and the specimen diameter (d) normalized by Burgers vector (b) followed the correlation of ¸i/G = 0.33(d/b)10.63. The size-dependent strength was reduced by cold-rolling, resulting in lower power-law exponents (0.2630.31) for the correlation in the cold-rolled specimens. The fine dislocation substructures introduced by the cold-rolling could be associated with the reduced size-dependent strength, which can be rationalized using the stochastic model of the dislocation source length in an assumption of homogenously distributed dislocations existing in the experimental micropillars. The inhomogeneous dislocation substructure with various dislocation cell sizes would contribute to a variation in the measured strength depending on the location, likely due to the probability of exiting the dislocation cell walls (local variation in dislocation density) in the micropillars fabricated on the cold-rolled Al samples. [doi:10.2320/matertrans.MT-L2023004]

DOI： 10.2320/matertrans.MT-L2023004

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Science and Engineering: A  

Owing to good formability, wrought Al alloys are used in a wide range of industries, including turbochargers in automobile engines. The development of Al alloys with increased high-temperature strength is necessary to improve the fuel efficiency of engines. In this study, a modified heat-resistant Al–Mg–Zn–Cu–Ni quinary alloy with superior high-temperature strength and creep rupture life at 200 °C (potential temperature in service for compressor radial impellers) was designed. The thermodynamic assessments provided a modified alloy composition of Al–5Mg–3.5Zn–2Cu–2Ni (at %) exhibiting α-Al phase in equilibrium with T-Al6Mg11Zn11 and Al3(Ni, Cu)2 phases at elevated temperatures. The experimental alloy showed granular T and Al3(Ni, Cu)2 phases often located on grain boundaries in the α-Al matrix, although the undissolved Al3Ni phase (formed in solidification) locally remained. Apart from the T phase, the η-Zn2Mg phase containing Cu element preferentially precipitated on grain boundaries. A large number of fine precipitates were dispersed homogeneously in the grain interior after the aging at 200 °C or 300 °C. Compared to the base alloy with a ternary composition of Al–5Mg–3.5Zn (at %) and conventional Al alloys, the designed quinary alloy (pre-aged at 200 °C for 10 h) showed a high strength at elevated temperatures above 200 °C. The creep-rupture life at 200 °C/105 MPa was remarkably extended to 665 h by the addition of Cu and Ni elements into the base ternary alloy. The rupture life was more than ten times longer than one (57 h) of the ternary alloys. The alloy modification based on the thermodynamic calculations provides an effective approach for designing lightweight Al alloys with superior high-temperature strength and creep rupture life.

DOI： 10.1016/j.msea.2022.144055

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Science and Engineering: A  

The aim of the present study was to identify the effect of solute Ni element on the plastic deformation and its thermal activation process of 18Cr ferritic stainless steels. Single-crystal micropillars with different diameters of approximately 2 and 5 μm were fabricated on the surface of Fe–18%Cr–Ni alloy sheets containing different contents of Ni (0–2 mass%). Compression tests were performed on the micropillars at different initial strain rates to investigate the strain rate sensitivity (m) of stress for the slip initiation and the specimen-size dependence of the m value. In micropillars with a small diameter of 2 μm, the Fe–18%Cr binary alloy specimen exhibited a relatively higher strain-rate sensitivity of initial slip stress (m = 0.12), whereas m was reduced to 0.01 by adding 2% Ni. The same trend was observed in micropillars with a larger size of approximately 5 μm. The experimental results were utilized to evaluate the activation volume of plastic deformation. The activation volumes of the Fe–18%Cr alloy and alloy containing 1% Ni followed the specimen-size dependence trend of activation volume in bcc metals; however, the alloy containing 2% Ni exhibited larger activation volumes, suggesting a different thermal activation process presumably due to the significant interaction that occurred between dislocations and solute Ni atoms in bcc solid-solutions.

DOI： 10.1016/j.msea.2022.144076

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Additive Manufacturing  

A Single laser scan was performed on a sintered WC/Co composite and the process conditions were optimized to realize a WC/Co two-phase microstructure in a WC/Co composite fabricated by laser powder bed fusion (L-PBF). Laser irradiation on the sintered WC/Co composites generated two different microstructural regions. One is composed of WC and Co phases (WC/Co two-phase region), and the other includes W2C and W3Co3C phases (WC decomposition region). In the L-PBF-fabricated WC/Co composites, these two microstructural regions are distributed in a complex manner and their fractions varies depending on the laser parameters. Using a convolutional neural network model that is trained with the micrographs of single-laser-scanned WC/Co composites, the fractions of the two microstructural regions in the WC/Co composites fabricated by the L-PBF under various laser conditions were quantified. Multiple linear regression analyses revealed that the laser power and spot size contribute more than the scan speed, which has been verified by numerical analysis based on the moving heat source model. A support vector machine (SVM) suggested that low laser power and low scan speed are required for suppressing the WC decomposition in the consolidated samples. The WC decomposition has been successfully suppressed in the samples fabricated under SVM-recommended conditions.

DOI： 10.1016/j.addma.2022.103089

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Science and Engineering: A  

Achieving both high strength and ductility is challenging in additive manufacturing of Al alloys using the laser powder bed fusion (L-PBF) process by altering the laser conditions to control the microstructural characteristics. The current work focuses on the influence of varying laser energy density (ED), which is adjusted by different sets of laser power (P) and scan speed (v), on the microstructure-tensile property relationships of the L-PBF-fabricated Al–2.5%Fe alloy under varying laser conditions (P = 204–230 W, v = 450–600 mm/s) with a fixed powder layer thickness (t = 30 μm) and hatch distance (h = 30 μm). With increasing ED (= P/v·t·h), a slight increase in the average size of the columnar α-Al grains was found in the experimental samples concurrently with a higher fraction of <001>-oriented grains. Nanosized particles of the Al6Fe phase with an increased tendency to interconnect were observed in the matrix inside the melt pool, and the θ phase formed within the submicron-sized cellular structure along the melt pool boundaries (MPBs). A low tensile ductility, induced by the local microstructural inhomogeneities across MPBs, was found in all specimens tensile-deformed along the building direction, which was characterized by a preference fracture along the MPBs. At higher applied ED, the tensile ductility of the experimental Al–2.5Fe alloy was significantly improved with only a slight decrease in tensile strength. The difference in concentration of Fe across the MPBs in the matrix was also moderately diminished, which is consistent with the reduced local difference in microhardness across the MPBs under higher ED conditions. Therefore, the present results demonstrate that local microstructural inhomogeneities across MPBs can be controlled by the laser conditions, thereby producing both high strength and good ductility in the L-PBF processed Al–Fe alloys.

DOI： 10.1016/j.msea.2022.143893

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Journal of Materials Processing Technology  

An Al alloy (A5052) sheet was joined with a carbon fiber-reinforced thermoplastic (CFRTP) sheet by hot pressing without melting the CFRTP sheet (that is, solid-state joining). A micro-structure was manufactured via laser irradiation of Al-Ti-C powders bedded on the A5052 sheet. The laser irradiation to Al-Ti-C powders generates numerous particle-shaped protrusions additively on the A5052 sheet, which facilitate the infiltration of CFRTP and mechanically interlock with the CFRTP sheet. To determine the optimal conditions for joining A5052 and CFRTP consisting of a polyamide 6 (PA6) matrix, the effects of joining temperature during hot pressing on the interfacial structure and joint strength were investigated. The maximum joint strength was attained at the joining temperature of 210 °C. At lower temperatures, PA6 was not sufficiently softened to infiltrate the micro-structure, resulting in lower joint strengths. At higher temperatures, carbon fibers (CFs) were exposed on the CFRTP surface and inhibited the penetration of PA6 and CFs into the micro-structure, thereby lowering the joint strength. To infiltrate PA6 and CFs into the micro-structure, hot pressing was performed in a gradient temperature field. The proposed process enabled appropriate infiltration of CFs and PA6 into the micro-structure and led to high and stable joint strength. It is expected that using the additively manufactured micro-structure approach proposed herein, the operating windows of various cutting-edge joining processes can be expanded to more moderate and lower energy conditions.

DOI： 10.1016/j.jmatprotec.2022.117629

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials  

The samples of the Al–15Fe (mass%) binary alloy that were additively manufactured by laser powder bed fusion (L-PBF) were exposed to intermediate temperatures (300 and 500◦C), and the thermally induced variations in their microstructural characteristics were investigated. The L-PBF-manufactured sample was found to have a microstructure comprising a stable θ-Al13Fe4 phase localized around melt-pool boundaries and several spherical metastable Al6Fe-phase particles surrounded by a nanoscale α-Al/Al6Fe cellular structure in the melt pools. The morphology of the θ phase remained almost unchanged even after 1000 h of exposure at 300◦C. Moreover, the nanoscale α-Al/Al6Fe cellular structure dissolved in the α-Al matrix; this was followed by the growth (and nucleation) of the spherical Al6Fe-phase particles and the precipitation of the θ phase. Numerous equiaxed grains were formed in the α-Al matrix during the thermal exposure, which led to the formation of a relatively homogenous microstructure. The variations in these microstructural characteristics were more pronounced at the higher investigated temperature of 500◦C.

DOI： 10.3390/ma15134497

Web of Science

Scopus

PubMed

その他リンク： https://www.mdpi.com/1996-1944/15/13/4497

担当区分：筆頭著者,　責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials and Design  

We examined the variation in the solidification microstructure of AlSi10Mg alloy powder over a wide range of cooling rates controlled by using the fast scanning calorimetry (FSC) technique. Two exothermic peaks derived from the primary solidification of the α-Al phases and the α-Al/Si eutectic reaction were detected. These exothermic peaks became broader and shifted to lower temperatures at higher cooling rates. Focus ion beam (FIB) milling enables microstructural characterization of AlSi10Mg powder solidified at controlled cooling rates above 102 °C·s−1 in the FSC equipment. The sample solidified at 4 × 104 °C·s−1 exhibited a fine microstructure consisting of a primary α-Al phase surrounded by lamellar-shaped Si phases. The fraction of the Si phase continuously decreased with increasing cooling rate, indicating higher content of solute Si element in the α-Al phase solidified at a higher cooling rate. The secondary dendrite arm spacing (λ) of the primary α-Al phase decreased in the sample solidified at a higher cooling rate (dT/dt). The relation follows a general equation of λ = A (dT/dt)-n (A: 38.4, n: 0.33) in wide range of cooling rate (10-1 ∼ 104 °C·s−1). The results were utilized to discuss the cooling rate of Al alloys during the laser powder bed fusion (L-PBF) process.

DOI： 10.1016/j.matdes.2022.110830

Scopus

その他リンク： https://www.sciencedirect.com/science/article/pii/S026412752200452X

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

DOI： 10.2464/jilm.72.246

Scopus

その他リンク： https://www.jstage.jst.go.jp/article/jilm/72/5/72_7205-T14/_article/-char/ja/

担当区分：筆頭著者,　責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

We have investigated microstructural characteristics and solute Si element in the α-Al (fcc) matrix of Al-12%Si binary alloy additive-manufactured by laser powder bed fusion (L-PBF) process in terms of different locations in the melt-pool structure (inside melt-pool or around melt-pool boundaries). Their variations by post heat-treatments at various temperatures were examined. The fraction of Si phase and lattice parameter of α-Al phase were quantified by XRD measurements combined with sample rotation and oscillation systems. In the L-PBF manufactured sample, the columnar α -Al phases contained highly concentrated Si element in solution (above 3 mol%) inside melt-pools, whereas the measured Si content was approximately 2 mol% in the relatively coarsened α-Al phase along melt-pool boundaries. The location dependence of solute Si content would be associated with a continuous change in growth rate of solid phase in solidification by local heating in the L-PBF process. The solute Si content was significantly reduced by heat-treatments and its location dependence appeared less pronounced. The as-manufactured sample exhibited a lower lattice parameter of α-Al phase with concentrated Si in solution in comparison with the heat-treated samples. The fraction of Si phase became higher in the heat-treated samples. These results were rationalized by microstructural change at elevated temperatures.

DOI： 10.2464/jilm.72.178

Scopus

その他リンク： https://www.jstage.jst.go.jp/article/jilm/72/5/72_7205-T08/_article/-char/ja/

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

Laser powder bed fused Al-10Si-0.4Mg (mass%) alloy exhibits low and anisotropic thermal conductivity. To elucidate dominant microstructural features generating the characteristic thermal conductivity, thermal conduction analysis was performed by an image-based finite element method (FEM) using scanning electron microscope (SEM) images. The serial sectioning images of as-fabricated and 300ºC/2 h heat treated Al-10Si-0.4Mg alloys were obtained by focused ion beam SEM (FIB-SEM) and were used for constructing three-dimensional models. The homogenization method was applied to calculate average thermal conductivity of these models. When the thermal conductivity of α-Al phase was set at the thermal conductivity of pure aluminum, calculated thermal conductivity of as-fabricated model was much higher than experimentally measured thermal conductivity of as-fabricated Al-10Si-0.4Mg alloy, indicating that α-Al phase in the as-fabricated Al-10Si-0.4Mg alloy had much lower thermal conductivity than pure aluminum. In addition, the anisotropy of thermal conductivity appeared only in the as-fabricated model in which the α-Al/Si interfacial thermal resistance was taken into account. These results were used for discussing dominant contributors of low and anisotropic thermal conductivity of laser additive manufactured Al-10Si-0.4Mg alloy.

DOI： 10.2464/jilm.72.164

Scopus

その他リンク： https://www.jstage.jst.go.jp/article/jilm/72/5/72_7205-T06/_article/-char/ja/

担当区分：筆頭著者,　責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Scripta Materialia  

This article reports an unexpected finding of the mechanical behavior of Al-12%Si alloy manufactured using the laser powder bed fusion (L-PBF) process. The as-manufactured specimen has a negative strain rate sensitivity of flow stress at an early stage of tensile deformation (below 3% in strain). The post heat-treated specimens exhibited a positive strain-rate sensitivity and none of these specimens exhibited a serrated stress-strain curve, indicating a mechanism different from the Portevin–LeChatelier effect. Transmission electron microscopy revealed the dynamic precipitation of the nano-sized Si-phase inside the supersaturated solid solution of the α-Al matrix in the as-manufactured specimen deformed at ambient temperatures. The dynamically precipitated Si phase interacted with the introduced dislocations, enhancing the flow stress during the early stages of plastic deformation. The dynamic precipitation could contribute to the negative strain-rate sensitivity of the flow stress at an early stage of tensile deformation (including the yield strength).

DOI： 10.1016/j.scriptamat.2022.114635

Scopus

担当区分：筆頭著者,　責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： doi.org/10.2320/materia.61.195

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Science and Engineering: A  

This study investigated the high-temperature strength of a hypereutectic Al–Fe binary alloy (Al–15%Fe) additive-manufactured by laser powder bed fusion (L-PBF). The L-PBF Al–15%Fe alloy exhibited superior yield strength to the other existing L-PBF processed alloys due to α-Al/Al6Fe eutectic structure with a nanoscale cellular morphology. The present results demonstrated the feasibility of using L-PBF processed Al–Fe alloys as high-temperature lightweight materials.

DOI： 10.1016/j.msea.2022.142782

Scopus

担当区分：最終著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：日本鉄鋼協会  

DOI： doi.org/10.2355/isijinternational.ISIJINT-2021-506

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Journal of Materials Science and Technology  

The present study addressed the change in the microstructure of Al–2.5 wt% Fe binary alloy produced using laser powder bed fusion (L-PBF) technique by thermal exposure at 300 °C, and the associated mechanical and thermal properties were systematically examined as well. Multi-semi-cylindrical patterns corresponding to melt pools in the microstructure were macroscopically observed for the as-manufactured sample. No change in the melt-pool morphology was observed after thermal exposure for 1000 h. Inside the melt pools, a large number of the nanoscale metastable Al6Fe phase particles were uniformly distributed inside columnar grains of the α-Al matrix containing concentrated solute Fe in supersaturation. The sequential formation and coarsening of stable θ-Al13Fe4 phases were observed upon exposure to a 300 °C environment, but a considerable amount of nano-sized metastable Al6Fe phases remained even after 1000 h. Furthermore, the thermal exposure continuously reduced the concentration of solute Fe atoms in the α-Al matrix. No significant grain growth was found in α-Al matrix after 1000 h owing to the pinning effect of the dispersed fine particles on grain boundary migration. These results demonstrate a sluggish change in microstructural morphologies of the Al–2.5 wt% Fe alloy. The quantified microstructural parameters addressed dominant strengthening contributions by the solid solution of Fe element and Orowan strengthening mechanism by fine Al–Fe intermetallics in the L-PBF-produced alloy. The high strength level was sustained even after being exposed to 300 °C for long periods. The superior balance of mechanical properties and thermal conductivity can be achieved in the experimental alloys by taking advantage of the various microstructural parameters related to the Al–Fe intermetallic phases and α-Al matrix.

DOI： 10.1016/j.jmst.2021.04.038

Scopus

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

This study was set to examine the fundamentals of solidification microstructure and room-temperature fracture toughness of different eutectic aluminum (Al) alloys strengthened by T-Al6Mg11Zn11 and/or β-Al3Mg2 intermetallic phases. The thermodynamic calculations for an Al-Mg-Zn ternary system assessed three alloy compositions of Al-22.5Mg-23.5Zn, Al-35.5Mg-2Zn and Al-34.5Mg-5Zn (mol%) corresponding to α-Al/T, α-Al/β and α-Al/T/β eutectic compositions, respectively. The designed alloys were prepared by different cast process for changing the cooling rate in solidification. The Al-22.5Mg-23.5Zn and Al-35.5Mg-2Zn alloys exhibited a number of fibrous α phase surrounded by of T-phase and β-phase matrix, respectively. The morphologies of eutectic microstructures were refined by high cooling rate in solidification. The three-phase microstructure of α, T and β phases was often observed in slowly solidified Al-34.5Mg-5Zn alloy, whereas only the α/β two-phase eutectic microstructure was observed in the rapidly solidified alloy sample. The indentation fracture method using Vickers indentation test was applied to measure the room-temperature fracture toughness of the experimental alloys prepared by mold-casting. The α/β two-phase eutectic alloys exhibited a low fracture toughness of 1.1 MPa·m0.5 in comparison with the α/T two-phase eutectic alloy. The lower fracture toughness would be responsible for the brittleness of β-phase matrix in the α/β two-phase eutectic alloys.

DOI： 10.2464/jilm.72.79

Scopus

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Journal of the Society of Powder Technology, Japan  

This paper introduces meso-scale structure synthesis on metal surfaces through reaction processes from raw metal powders. The mesostructures are applied to metal/polymer anchor joining. The first topic is the synthesis of Fe-based porous structure on Fe substrate through the combustion reaction of the Fe-Ti-B system. The structure could be controlled in view of the phase equilibria at the maximum temperature of the reaction. A Fe/epoxy resin joint via the porous structure exhibits high tensile strength in a direction perpendicular to the joint interface. The second topic is the fabrication of mesostructure protruded on an Al alloy surface by laser scanning on Al-Ti-C powders. The mesostructural morphology is related to the formation of TiC and Al3Ti phases, which can be understood based on the solidification sequence after the laser irradiation. An Al alloy/CFRTP joint via the mesostructure exhibits high joint strength compared with previously reported similar anchor joints.

DOI： 10.4164/sptj.59.511

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：ISIJ International  

The influence of different stabilizing elements (Nb, Ti and Zr) which are added to stabilize interstitial elements in the ferrite matrix on the ductile-brittle transition temperature (DBTT) of 18Cr ferritic stainless steels was systematically investigated at different temperatures ranging from −25°C to 75°C. Hot-rolled sheets of 18 mass% Cr ferritic stainless steels containing a trace amount (0.1 atomic%) of Nb, Ti or Zr were studied. The added stabilizing elements formed precipitates of carbides/nitrides in all the steels tested in the present study. The particle diameter of the precipitates observed in the Nb-added steel was much smaller than those in the other steels. The measured DBTTs of the Base steel and the Nb-added, Ti-added and Zr-added steels were 39°C, −3°C, 39°C and 11°C, respectively. Although initiation of cleavage cracks in each steel occurred independent of the kind of stabilizing element, the Nb-added steel exhibited a relatively higher Charpy impact value due to ductile plastic deformation following cleavage crack initiation, resulting in a lower DBTT (superior impact toughness). The occurrence of plastic deformation in the Nb-added steel is considered to be due to the fine carbide and/or nitride precipitates which were homogenously distributed in the material. Detailed analyses of the fracture surfaces were also performed for the other steels, and the results were used as a basis for discussing the effects of each stabilizing element on the DBTT of 18Cr ferritic stainless steels in terms of the precipitation morphologies observed in the ferrite matrix.

DOI： 10.2355/isijinternational.ISIJINT-2021-506

Scopus

担当区分：筆頭著者,　責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

DOI： 10.2464/JILM.72.381

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Transactions  

In the present study, we investigated the effects of Cu or Ni additions on the precipitation of intermetallic phases in the heat-resistant aluminum alloy with a ternary composition of Al5Mg3.5Zn (mol%). The quaternary alloys with 1 mol%Cu or 1 mol%Ni content were solution-treated at 480°C and subsequently aged at 300°C for different periods. Both Cu and Ni additions have a slight effect on the agehardening of these alloys at 300°C. The added Cu element partitioned into not only the T-Al6Mg11Zn11 phase but

DOI： 10.2320/matertrans.MT-L2021021

Scopus

その他リンク： https://www.jstage.jst.go.jp/article/matertrans/63/4/63_MT-L2021021/_article/-char/ja/

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Journal of Materials Science  

Carbon nano-materials are widely used as reinforcing materials for aluminum-based composites due to their excellent metallurgical properties. This study presents an approach for manufacturing Al/C composites utilizing a high energy ball milling and laser powder bed fusion (LPBF) process. We prepared Al/C60 and Al/MWCNT composites under 25 different conditions to observe their microstructure and mechanical property trends according to laser power and scan speed. The relative density of LPBFed composites increased as the energy density increased due to the oxide layer present on the aluminum surface and the high laser reflectance. It was found that, as the energy density increased, the increase in nanohardness and elastic modulus of the LPBFed composites was due to the high relative density. However, the high laser power condition of 179 W resulted in the softening of materials due to grain coarsening, resulting in a decrease in nanohardness and elastic modulus. Under the same laser conditions, the nanohardness of the LPBFed Al/2 vol.% MWCNT composites was approximately 0.5 GPa higher than that of the LPBFed Al/1 vol.% C60 composites, which is explained by the high relative density and grain refinement strengthening.

DOI： 10.1007/s10853-022-07119-6

Scopus

その他リンク： https://link.springer.com/article/10.1007/s10853-022-07119-6

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

The effect of Cu or Ni addition on creep properties of a heat-resistant aluminum (Al) alloy (with a composition of Al-5Mg-3.5Zn (mol%)) strengthened by precipitates of T-Al6Mg11Zn11 intermetallic phase was investigated. The quaternary alloys with various Cu contents (0.25-3 mol%) or Ni contents (0.5-2 mol%) were solution-treated at 470 °C and then aged at 200°C for 10 hours. The creep tests were conducted using the heat-treated specimens at 200°C under 105 MPa. Both Cu and Ni additions increased the creep rupture time. The 1 mol% Cu added alloy exhibited the longest creep rupture time due to the enhanced precipitation of the refined intragranular phases (T or MgZn2 phases). However, more than 2 mol% Cu addition led to the transition of T phase to S-Al2CuMg phase formed on grain boundaries. The phase transition might have a detrimental effect on creep rupture time. In the Ni-added alloy specimen, the creep rupture time became longest when 1 mol% Ni was added. The added Ni element promoted the formation of the Al3Ni phase on the grain boundaries, resulting in the suppression of connecting cavities formed on grain boundaries in creep deformation.

DOI： 10.2464/JILM.72.473

Scopus

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy  

In the laser beam powder bed fusion (PBF-LB) processes, laser parameters need to be customized for fabricating dense components. Al-Si alloys are representative Al alloys used for the PBF-LB processes. The Al-Si alloys fabricated by the PBF-LB processes exhibit characteristic microstructures and mechanical properties, which are affected by the laser parameters. This paper describes the effect of laser conditions on the relative density, microstructure, and mechanical properties of Al-12Si (mass%) alloy fabricated by the PBF-LB process. The first topic is a machine-learning-assisted exploration of laser parameters (laser power and scan speed) for fabricating dense Al-12Si alloy parts. Using a neural network model, the laser condition range for fabricating dense Al-12Si alloy parts is predicted. A methodology for accurately predicting the laser condition range for fabricating dense components is introduced. The second topic is controlling the microstructures and mechanical properties of the dense Al-12Si alloys. Variations in α-Al crystal grain size/orientation, the width of primary α-Al phase, and solute Si content in α-Al matrix with laser conditions are introduced. The changes in mechanical properties with laser conditions and correlation with microstructural features are also described.

DOI： 10.2497/jjspm.69.417

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Additive Manufacturing Letters  

In order to manage both the strength and ductility of Al–Si alloys additively manufactured by laser powder bed fusion (L-PBF), an attempt was made to introduce nanoscale precipitates within the α-Al (fcc) supersaturated solid solution using the L-PBF manufactured Al–12%Si alloy by artificial aging treatments. The aging treatment at 120°C improved both the tensile strength and ductility (total elongation) of the L-PBF manufactured specimen. The simultaneous strength–ductility enhancement is due to the homogeneously distributed nanoscale Si precipitates that enhanced the strain hardening. These results provide new insights for overcoming the strength-ductility trade-off in the L-PBF manufactured Al alloys.

DOI： 10.1016/j.addlet.2021.100008

Scopus

担当区分：筆頭著者,　責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Intermetallics  

This study was undertaken to understand the fundamentals of T-Al6Mg11Zn11 intermetallic phase precipitation in heat-resistant Al–Mg–Zn ternary alloys, with the goal of further strength improvements. The thermodynamic assessment involved three alloy compositions, Al–4Mg–4.5Zn, Al–5Mg–3.5Zn, and Al–7Mg–1.5Zn (at%), with the T phase in a fixed fraction (approximately 6–7.5%) in equilibrium with the α-Al phase at 300 °C. The alloy compositions were set on different tie-lines between the α-Al and T phases in the two-phase region, resulting in varied compositions of each phase. In the three experimental alloys aged at 300 °C, the T phase precipitated on the grain boundaries of the α-Al matrix, and granular precipitates were homogeneously dispersed intragranularly. There was no significant difference in the precipitation morphology. It was demonstrated that the lattice parameters of the T and α-Al phases could be controlled based on the alloy composition and applied heat treatments. However, the lattice parameters have no significant effect on the precipitation morphologies of the thermodynamically stable T phase in the Al–Mg–Zn ternary alloys. The Zn-rich Al–4Mg–4.5Zn alloy exhibited a pronounced softening behavior after 10 h of aging due to the enhanced coarsening of precipitates in the α-Al matrix. The thermal instability of the precipitates was responsible for the transformation sequence from the initially formed metastable phases (η-Zn2Mg associated phases) to the stable T phase. These results provided a fundamental insight that alloy strengthening by introducing thermodynamically stable intermetallic phases is essential for sustaining the strength of heat-resistant Al–Mg–Zn ternary alloys after long-term treatment at elevated temperatures.

DOI： 10.1016/j.intermet.2021.107364

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Additive Manufacturing  

To elucidate the possibility of controlling the microstructure and mechanical properties of Al–Si alloys additive-manufactured by laser powder bed fusion (L–PBF), the relationship among the laser conditions, microstructural characteristics (crystal grain, cellular microstructure, and solute Si in α-Al matrix), and tensile properties of L–PBF manufactured AlSi12 alloy samples was investigated. The crystal grain size and fraction of <001> oriented α-Al crystal grains toward the building direction increased as the laser power became higher and scanning velocity became slower. The width of cellular microstructure (sub–cell size) where the primary α-Al phase was surrounded by α-Al/Si eutectic microstructure increased as the laser power became higher and scanning velocity became slower. The refinement of microstructure was attributed to the solidification under high cooling rate, which was achieved by low laser power and high scanning velocity. The area fraction of Si phase analyzed from FE–SEM images tended to decrease as the laser power became higher and scanning velocity became slower, suggesting the possibility of solute Si concentration in α-Al matrix controlled by laser conditions. The STEM/EDS analysis revealed high concentration of solute Si in the α-Al matrix (above a solubility limit of 1.5 mol% in the Al–Si binary system) of L–PBF manufactured AlSi12 alloy samples and its concentration became higher in the sample manufactured using a higher laser power. The tensile tests of as–built AlSi12 specimens fabricated under various laser conditions were also performed. High strength and high ductility tended to be achieved when high power laser was applied in slow laser scanning velocity. The 0.2% proof stress was relatively higher when the laser scanning velocity was faster. The mechanical properties correlated with crystal grain size and sub–cell size rather than solute Si in the α-Al matrix. These results provide new insights to control mechanical performance of AlSi12 alloy via L–PBF processing parameters.

DOI： 10.1016/j.addma.2021.102383

Scopus

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials  

The precipitation of intermetallic phases and the associated hardening by artificial aging treatments at elevated temperatures above 400◦ C were systematically investigated in the commer-cially available AC2B alloy with a nominal composition of Al–6Si–3Cu (mass%). The natural age hardening of the artificially aged samples at various temperatures was also examined. A slight increase in hardness (approximately 5 HV) of the AC2B alloy was observed at an elevated temperature of 480◦ C. The hardness change is attributed to the precipitation of metastable phases associated with the α-Al15 (Fe, Mn)3 Si2 phase containing a large amount of impurity elements (Fe and Mn). At a lower temperature of 400◦ C, a slight artificial-age hardening appeared. Subsequently, the hardness decreased moderately. This phenomenon was attributed to the precipitation of stable θ-Al2 Cu and Q-Al4 Cu2 Mg8 Si6 phases and their coarsening after a long duration. The precipitation sequence was rationalized by thermodynamic calculations for the Al–Si–Cu–Fe–Mn–Mg system. The natural age-hardening behavior significantly varied depending on the prior artificial aging temperatures ranging from 400◦ C to 500◦ C. The natural age-hardening was found to strongly depend on the solute contents of Cu and Si in the Al matrix. This study provides fundamental insights into controlling the strength level of commercial Al–Si–Cu cast alloys with impurity elements using the cooling process after solution treatment at elevated temperatures above 400◦ C.

DOI： 10.3390/ma14237155

Web of Science

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier Ltd.  

In this study, an attempt is made to control the WC-Co two-phase microstructures by laser powder-bed fusion (LPBF) process using cemented carbide powders with different compositions of WC-25Co (mass%) and WC-17Co (mass%) and post heat-treatment at 1380 °C. The as-built cemented carbide samples had different microstructures from those of the cemented carbides fabricated by conventional manufacturing methods. The microstructures of the as-fabricated WC-25Co and WC-17Co cemented carbides were characterized by two types of regions. Region 1 consisted of W2C and W3Co3C phases, including numerous pores and defects. Region 2 consisted of WC and Co phases. Post heat-treatment of the LPBF-built WC-25Co sample at 1380 °C led to the formation of a defect-free WC-Co two-phase microstructure. In contrast, the W3Co3C phase remained in the LPBF-built WC-17Co sample even after heat treatment. The addition of carbon to the WC-17Co powder prevented the formation of the W3Co3C phase in the cemented carbide processed by LPBF and subsequent heat treatments. The addition of carbon to the WC-17Co powder had a slight effect on the hardness of as-fabricated samples, but reduced the hardness of heat-treated samples. The reduced hardness was attributed to the increased volume fractions of the WC and W3Co3C phases.

DOI： 10.1016/j.matdes.2021.110034

Scopus

その他リンク： https://www.sciencedirect.com/science/article/pii/S026412752100589X

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Materials Science and Engineering A  

The effects of a trace amount (~0.1 at.%) of added stabilizing elements (Nb, Ti, and Zr) on the tensile properties of 18Cr ferritic stainless steel sheets at strain rates ranging from 10−3–102 s−1 (from ordinary quasi-static deformation to dynamic deformation) were investigated. The additional Ti or Zr elements formed coarse carbide or nitride precipitates, which consumed interstitial solute elements (C and/or N) in the ferrite matrix. In the Nb-added steel, however, only fine NbN precipitates with a few hundred nanometers in size were observed locally, implying a small amount of solute Nb in the ferrite matrix. Ti or Zr additions had only a slight effect on the deformation resistance of 18Cr ferritic steel sheets and strain rate sensitivity (m) of the flow stress, however, the Nb addition increased the deformation resistance and significantly reduced the strain rate sensitivity. The measured activation volume (v*) values of the Ti- and Zr-added steels (62 b3 and 66 b3) were almost equivalent to one of the 18Cr base steel (64 b3). This result suggested that a general thermally activated process for screw dislocation motion is controlled by double-kink nucleation, which is slightly affected by Ti or Zr additions. The high v* value (106 b3) of the Nb-added steel indicated that the thermally activated process of plastic deformation would be associated with the substitutional solute Nb atoms (act as short-range obstacles) interacting with the moving dislocations. These results showed that the Nb element played a distinct role in plastic deformation from the other stabilizing elements of Ti and Zr.

DOI： 10.1016/j.msea.2021.141866

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Scripta Materialia  

Imitating crystal structures offers new avenues to design lattice structures composed of unit cells with nodes (act as atoms) and struts (act as atomic bonds). We found out unique dual plateau regions in the stress–strain curves of lattice structures inspired by topologically close-packed (TCP) structure of C15 Laves phase (AB2-type intermetallic compounds) and manufactured via the laser powder bed fusion. X-ray computed tomography of compressively deformed lattice structures as well as finite element analysis revealed that the existence of two kinds of units with different relative density caused the dual plateau regions. In addition, the C15 lattice structures exhibited a hybrid deformation mode of bending- and stretch-dominated deformations and can absorb high total energy of 5.0 MJ·m−3 in two stress levels.

DOI： 10.1016/j.scriptamat.2021.114003

Scopus

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier B.V.  

DOI： 10.1016/j.jajp.2021.100068

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier B.V  

DOI： 10.1016/j.msea.2021.141459

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：MDPI  

DOI： 10.3390/cryst11030320

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：John Wiley & Sons, Inc.  

DOI： 10.1002/adem.202001284

DOI： 10.1002/adem.202170017

その他リンク： https://onlinelibrary.wiley.com/doi/10.1002/adem.202170017

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier B.V.  

DOI： 10.1016/j.msea.2020.140591

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier Ltd.  

DOI： 10.1016/j.matdes.2020.109416

記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier B.V.  

DOI： 10.1016/j.jmatprotec.2020.116843

Web of Science

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier B.V.  

DOI： 10.1016/j.msea.2021.140861

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Elsevier B.V.  

DOI： 10.1016/j.msea.2020.140455

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（国際会議プロシーディングス）   出版者・発行元：Trans Tech Publications Ltd  

DOI： 10.4028/www.scientific.net/MSF.1016.1175

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（国際会議プロシーディングス）   出版者・発行元：Trans Tech Publications Ltd  

DOI： 10.4028/www.scientific.net/MSF.1016.826

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmbbm.2020.104130

担当区分：責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Keikinzoku/Journal of Japan Institute of Light Metals  

In the present study, we investigated the effects of Cu or Ni additions on the precipitation of intermetallic phases in the heat-resistant aluminum alloy with a ternary composition of Al-5Mg-3.5Zn (mol%). The quaternary alloys with 1 mol%Cu or 1 mol%Ni content were solution-treated at 480 °C and subsequently aged at 300 °C for different periods. Both Cu and Ni additions have a slight effect on the age-hardening of these alloys at 300 °C. The added Cu element partitioned into not only T-Al6Mg11Zn11 phase but η-Zn2Mg phase precipitated in the α-Al matrix. The observed Cu enrichment in the precipitates of T phase indicated high stability of T phase in the Al-Mg-Zn-Cu quaternary system, which was different from the results of thermodynamic calculations using the existing database. The added Ni element enhanced the formation of fine Al3Ni phase located at grain boundaries and slightly influenced the precipitation of T phase in grain interior. These results provided new insights to design novel heat-resistant Al alloys using the Al-Mg-Zn-Cu-Ni system.

DOI： 10.2464/jilm.71.275

Scopus

その他リンク： https://www.jstage.jst.go.jp/article/jilm/71/7/71_710701/_article/-char/ja/

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.3390/cryst10111007

その他リンク： https://www.mdpi.com/2073-4352/10/11/1007

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.intermet.2020.106892

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.addma.2020.101308

Web of Science

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.intermet.2020.106881

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.3390/ma13183927

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.addma.2020.101436

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.3390/ma13132902

Web of Science

その他リンク： https://www.mdpi.com/1996-1944/13/13/2902

担当区分：筆頭著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2497/jjspm.67.313

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.3390/ma13112487

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/isijinternational.ISIJINT-2019-448

Web of Science

その他リンク： https://www.jstage.jst.go.jp/article/isijinternational/60/4/60_ISIJINT-2019-448/_article/-char/ja

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.3390/ma13051238

Web of Science

その他リンク： https://www.mdpi.com/1996-1944/13/5/1238

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.11283/jlwa.58.102s

担当区分：筆頭著者,　責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.addma.2020.101152

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/matertrans.MT-M2019237

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmatprotec.2019.116388

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2020.139000

担当区分：責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmst.2019.06.015

Web of Science

担当区分：筆頭著者,　責任著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2019.138710

担当区分：筆頭著者   記述言語：日本語  

DOI： https://doi.org/10.2497/jjspm.66.573

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2019.138330

Web of Science

担当区分：筆頭著者   記述言語：日本語  

DOI： 10.11279/jfes.91.612

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2019.138247

Web of Science

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1002/adem.201900571

担当区分：筆頭著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/tetsutohagane.105.675

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.apt.2019.06.024

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/tetsutohagane.TETSU-2018-147

Web of Science

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/tetsutohagane.TETSU-2018-146

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.intermet.2019.03.011

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.addma.2019.04.018

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.14957/fgms.33.38

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmatprotec.2019.02.012

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2464/jilm.69.93

担当区分：筆頭著者,　責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan  

DOI： 10.2355/tetsutohagane.TETSU-2018-064

Scopus

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2018.10.034

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jallcom.2018.08.211

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmatprotec.2018.09.010

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1557/adv.2019.153

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記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1557/adv.2019.107

Web of Science

出版者・発行元：Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan  

DOI： 10.2355/tetsutohagane.TETSU-2018-150

Scopus

担当区分：筆頭著者,　責任著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy  

DOI： 10.2497/jjspm.66.573

Scopus

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.matdes.2018.08.005

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.3390/met8060440

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmatprotec.2018.06.010

Scopus

担当区分：筆頭著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2464/jilm.68.250

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

We designed two types of Al-based alloy composites reinforced by η-Zn2Mg (hexagonal) and T-Al6Mg11Zn11 (cubic) intermetallic phases using monovariant eutectic reactions in the Al–Mg–Zn ternary system and then attempted to fabricate them using solidification. Thermodynamic assessment revealed two alloy compositions of Al–18Mg–36Zn and Al–22.5Mg–23.5Zn (at%) with the α-Al (fcc) phase reinforced with high fractions (>50%) of the η and T phases. Both alloys exhibited fine two-phase eutectic microstructures consisting of α/η and α/T phases, respectively. The morphology of the α-Al phase in the eutectic colonies varied from lamellae to fibers upon changing the neighboring intermetallic phase. These eutectic microstructures exhibit high stability at an elevated temperature of 300 °C. In addition, the size and spacing of the α-Al phase could be controlled by changing the cooling rate during solidification. The fabricated composites exhibited high hardness values exceeding 220 HV, which were much superior to those of conventional Al alloys. The calculated solidification path and component partitioning in the liquid phase during solidification provided insights into the solidification segregation of Zn element in the Al–18Mg–36Zn alloy. The Zn-enriched regions would enhance the local microstructural change at elevated temperatures, which confirmed by the microstructural observations of the alloy exposed at 300 °C

DOI： 10.1016/j.intermet.2018.01.018

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.jmatprotec.2017.10.054

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.matchar.2017.11.052

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/isijinternational.ISIJINT-2018-036

Web of Science

担当区分：筆頭著者   記述言語：日本語  

DOI： 10.2464/jilm.67.571

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2464/jilm.67.582

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2017.08.029

Web of Science

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

Porous metals show some unique properties, which bulk metals cannot exhibit. Especially, iron-based porous metals are expected to be applied to structural components because of their high strength, high rigidity, low material cost and so on. In this research, we synthesized porous Fe/TiB2 composites by Fe-Ti-B combustion reaction. Iron, titanium and boron powders were blended to synthesize 30 to 60vol%TiB2 particles in Fe matrix after the combustion synthesis reaction. Four kinds of iron powders (powder size: < 53 μm, < 150 μm, 600 μm and 850-1000 μm) were used. The blended powder was heated to induce the combustion synthesis reaction. When < 53 μm and < 150 μm iron powders were used, irregular shaped and open pores were formed. On the other hand, when 600 μm and 850-1000 μm iron powders were used, spherical pores whose sizes and shapes were similar to those of iron powders were formed

DOI： http://doi.org/10.2497/jjspm.64.288

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.msea.2017.05.015

Web of Science

記述言語：日本語   掲載種別：研究論文（学術雑誌）   出版者・発行元：Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy  

DOI： 10.2497/jjspm.64.288

Scopus

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

In the present study, we have attempted to produce the porous Ti–Al intermetallic based alloys by pressure-sintering of the elemental powders of Ti and Al through a combustion reaction, with a NaCl space holder to achieve the development of a highly porous structure. The powders of Ti (particle size: <45 μm) and Al (particle size: <45 μm) were mixed to various total compositions of Ti–0-40 Al (at.%), and NaCl (particle size: 300-400 μm) was mixed with the Ti/Al powder to give a highly porous structure. The mixed powder was sintered at 700 oC under a constant pressure of 30 MPa to form cylindrical specimens with a diameter of 20 mm. The soaking of the specimens in pure water allows for the removal of NaCl (with a volume fraction of 60 %) and the formation of the pores to achieve a controlled relative density of 0.4. The present process can produce porous Ti–Al alloys with various compositions. In as-sintered Ti–Al specimens, an inhomogeneous microstructure consisting of Ti particles surrounded by the a Ti–Al alloy layer (various Ti–Al intermetallic phases) was observed. The as-sintered specimens exhibited the brittle behavior under compression, which is independent of their Al content. However, in a Ti–20Al alloy heat-treated at 1300 °C, a nearly Ti3Al single-phase microstructure appeared in the porous specimen. The heat-treated porous Ti–20Al alloy shows both a high plateau-strength level of approximately 100 MPa and a high plateau-end strain over 50%, resulting in a high absorption energy. The present results demonstrate that controlling the microstructure for the formation of the Ti3Al single-phase would be an effective method to achieve high energy absorption capacity of the porous Ti–Al alloy.

DOI： 10.1557/adv.2017.123

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

The three-phase, (Mo,Nb)ss/(Mo,Nb)5Si3/(Mo,Nb)5SiB2, Bcc/T1/T2 microstructures that develop in Mo–Nb–Si–B alloys have been examined in arc cast and directionally solidified samples to identify the phase sequencing during solidification. A Mo-32.6Nb-19.5Si-4.7B (at.%) alloy was directionally solidified using an optical floating zone (OFZ) furnace in a flowing Ar gas atmosphere at a constant growth rate of 10 mm/h. The microstructure of the directionally solidified alloy is characterized by an elongated T2 phase surrounded by bcc and T1 phases with an interwoven morphology From the evaluation of the microstructures in arc cast ingots of several alloys at a constant 32.6 at%Nb composition, the path of the liquidus valleys with decreasing temperature has been determined to intersect at a common point that establishes the solidification reaction as a eutectic. The incorporation of the experimental results into a computational thermodynamic analysis provides insight on the partitioning of components within each phase during solidification

DOI： doi:10.1016/j.intermet.2016.01.001

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： http://dx.doi.org/10.1016/j.msea.2016.03.038

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.intermet.2015.11.003

担当区分：筆頭著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/tetsutohagane.TETSU-2015-063

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/isijinternational.ISIJINT-2015-441

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.intermet.2015.07.011

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/isijinternational.55.1454

Web of Science

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： DOI: 10.1557/opl.201 .

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.intermet.2014.06.003

Web of Science

担当区分：筆頭著者   記述言語：日本語   掲載種別：研究論文（学術雑誌）  

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

We have examined the growth kinetics of Fe-Zn intermetallics layers formed on Fe-1.5Mn (α-Fe single phase) and Fe-3.5Mn-0.1C (γ-Fe+α-Fe two phase) steel sheets dipped in pure Zn melt at 460 ºC. In an early stage of dipping, FeZn13-ζ phase layer is initially formed and its thickness slightly increases with increasing dipping time till about 10 s, and then all Fe-Zn intermetallics layers (ζ, δ1, Γ) grow following a parabolic law. The growth kinetics can be recognized in both steels. This result demonstrates a slight effect of steel microstructure on the formation of Fe-Zn intermetallics layers. The composition analysis revealed a significant Fe dissolution into pure Zn melt in an early stage of dipping. The supersaturated Fe in Zn melt would provide the driving force for the crystallization of ζ phase layer on steel sheets. The continuous layer of ζ phase would control Fe diffusion for the following growth of the other Fe-Zn intermetallics layers.

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

Creep of carbon free Fe-20Cr-30Ni-2Nb (at.%) steels strengthened by Fe2Nb Laves phase on grain boundaries has been examined in air and steam atmospheres at 1073 K/70 MPa. Sufficiently covering grain boundaries by stable Laves phase can reduce the creep rate, resulting in a significant extension of the creep rupture life without a loss of creep ductility in steam atmosphere as well as air. This effect becomes remarkable in higher area fractions of Laves phase on grain boundaries (ρ) than 80%. The creep rupture strain slightly decrease by steam atmosphere, which would be associated with the interglanular oxidation and its related cracks propagation along grain boundaries enhanced by steam atmosphere in the creep acceleration stage. Its effect can be suppressed by covering grain boundaries by Laves phase (increasing ρ). Therefore, Grain Boundary Precipitation Strengthening by stable Laves phase is a key mechanism for use of materials for boiler tubes in the innovative advanced ultra-super critical (A-USC) thermal power plants to be operated above 973 K.

担当区分：筆頭著者   記述言語：英語  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.scriptamat.2012.12.019

Web of Science

担当区分：筆頭著者   記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： DOI: 10.1557/opl.2012.

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.scriptamat.2011.01.026

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1088/1742-6596/240/1/012015

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.matlet.2009.05.021

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.scriptamat.2008.12.018

Web of Science

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1016/j.scriptamat.2008.09.002

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記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/matertrans.MD200809

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

掲載種別：研究論文（大学，研究機関等紀要）  

掲載種別：研究論文（大学，研究機関等紀要）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1007/s10853-008-2971-9

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1007/s10853-008-2972-8

Web of Science

記述言語：日本語  

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

アルミニウム誘起結晶化法(AIC法)により形成された多結晶シリコン(Si)薄膜の形成挙動を透過電子顕微鏡(TEM)内その場加熱観察法等の微細構造解析手法により調査した.走査透過電子顕微鏡(STEM)を用いたエネルギー分散型X線分光法(EDS)分析により,400℃で10時間の熱処理でアモルファスSi(a-Si)とAlが完全に層交換することが確認できた.さらに,200℃での熱処理途中段階でのTEM内その場加熱観察ならびにEDS線分析により,SiとAlが各層内に共存することを明らかにできた.これらの結果より,AICによるa-Siの結晶化はSiの非平衡状態でのAlとの固溶を経由して起こると考えられる.

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/matertrans.MRA20073121

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記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/matertrans.ME200715

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記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

記述言語：日本語   掲載種別：研究論文（大学，研究機関等紀要）  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

掲載種別：研究論文（学術雑誌）  

掲載種別：研究論文（学術雑誌）  

掲載種別：研究論文（学術雑誌）  

DOI： 10.2355/isijinternational.48.1114

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1166/jnn.2007.073

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記述言語：日本語  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

記述言語：日本語  

記述言語：日本語  

記述言語：日本語   掲載種別：研究論文（大学，研究機関等紀要）  

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

掲載種別：研究論文（学術雑誌）  

掲載種別：研究論文（学術雑誌）  

記述言語：日本語  

記述言語：日本語  

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

Al誘起結晶化法(AIC法)は,低温で多結晶シリコン(Si)薄膜の作製が可能なプロセスとして注目されている.本研究では,種々の膜厚比で蒸着させたAlとアモルファスSi(a-Si)を対象に低温熱処理による結晶化過程について検討した.その結果,多結晶Siは最初に蒸着したAlの膜厚分だけデンドライト状に成長することが明らかになった.本研究の条件では,a-SiとAlを1:1で蒸着させた試料が多結晶Siの膜の形成状態が良好であった.また,TEM内その場加熱観察を行った結果,a-Si中にAlが固溶している様子が観察され,Siは非平衡状態のa-Si/Al固溶体を経由して結晶化することが示唆された.

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

記述言語：日本語   掲載種別：研究論文（学術雑誌）  

  In this study, the energy and atomic structure of the <110> symmetric tilt boundaries in palladium were calculated using a molecular dynamics (MD) method and the electronic structures of hydrogen in the bulk and at the grain boundaries were calculated using discrete-variational Xα (DV-Xα) molecular orbital cluster calculaion by solving Hartree-Fock-Slater equation.    The result of MD simulation revealed that the energy of the <110> symmetric tilt boundary of palladium depended on the misorientation angle and that there were large energy cusps at the misorientation angles which correspond to the {111}Σ3 and {113}Σ11 symmetric tilt boundaries. The atomic structure of all <110> symmetric tilt boundaries could consist of the combination of the {331} Σ19, {111}Σ3 and {113}Σ11 structural units and {110}Σ1 and {001}Σ1 single crystal units.    The result of DV-Xα molecular orbital cluster calculation showed that the interstitial hydrogen atoms induced the palladium-hydrogen chemical bond which had a different energy level from the palladium-palladium bond. The component of the palladium-hydrogen bond at the grain boundaries was similar to those in the bulk palladium. It is clarified that electronic structure near the grain boundary is different from that in the perfect crystal.

記述言語：英語   掲載種別：研究論文（学術雑誌）  

DOI： 10.1143/JJAP.44.4770

Web of Science

記述言語：日本語  

掲載種別：研究論文（学術雑誌）  

掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/matertrans.45.2099

記述言語：英語   掲載種別：研究論文（学術雑誌）  

Web of Science

掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/jinstmet.68.240

掲載種別：研究論文（学術雑誌）  

DOI： 10.2320/matertrans.45.1687

掲載種別：研究論文（学術雑誌）  

記述言語：日本語  

記述言語：日本語  

記述言語：英語   掲載種別：研究論文（学術雑誌）  

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開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年11月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年9月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年6月

記述言語：英語   会議種別：口頭発表（一般）  

開催地：Vienna (Online)   国名：オーストリア共和国  

その他リンク： https://www.galvatech2020.org/

開催年月日： 2021年6月

記述言語：日本語  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年6月

記述言語：日本語  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年6月

記述言語：日本語  

開催地：オンライン開催   国名：日本国  

開催年月日： 2021年5月

記述言語：日本語   会議種別：ポスター発表  

開催地：オンライン開催  

その他リンク： https://www.jilm.or.jp/convention/index

開催年月日： 2021年5月

記述言語：日本語   会議種別：ポスター発表  

開催地：オンライン開催  

その他リンク： https://www.jilm.or.jp/convention/index

開催年月日： 2021年5月

記述言語：日本語   会議種別：ポスター発表  

開催地：オンライン開催  

その他リンク： https://www.jilm.or.jp/convention/index

開催年月日： 2021年5月

記述言語：日本語   会議種別：口頭発表（一般）  

開催地：オンライン開催  

開催年月日： 2021年5月

記述言語：日本語   会議種別：口頭発表（一般）